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76 4 Intoxicated by Implants. 1 mol L1 H3PO4 soln Development solventMobile phase AcetoneCHCl3 (5:95 to 15:85) Tolueneethyl acetate formic acid (5:4:1) or benzeneCH3OHacetic acid (18:1:1, two sequential developments) H2OCH3CNacetic acid (99:99:2) Stationary phase Silica gel Silica gel C18 column Clean-up method NaHCO3 diatomaceous earth column NaHCO3 diatomaceous earth column C18 SPE Detection limit, LOD (ðg kg1)Additional information LOD not specified (IUPACAOAC method) LOD not specified 10.
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